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Publications in 1985


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The numbers following each publication are linked to the structures reported in the publication.

1985
  1. Durfee, L. D.; Latesky, S. L.; Rothwell, I. P.; Huffman, J. C.; Folting, K.: Chemical and Electrochemical Reduction of Titanium(IV) Aryloxides.  Inorg. Chem. 1985, 24, 456973.
    83927, 84913
  2. Chisholm, M. H.; Eichhorn, B. W.; Huffman, J. C.: Reaction Between bis(benzyl)tetraisopropoxyditungsten(W.tplbnd.W) and but2yne: W2(CH2Ph)2(OCHMe2)4(.eta.2C2Me2)2 and W2(H)(OCHMe2)4(.mu. CPh)(.mu.C4Me4). A Terminal Metal Hydride with a Proton NMR Resonance 20 ppm Downfield of Tetramethylsilane.  J. Chem. Soc., Chem. Commun. 1985, 8613.
    84076
  3. Seela, J. L.; Huffman, J. C.; Christou, G.: Preparation, Structure, and Properties of [NEt4][Mn(edt)2(Him)] (H2edt = ethane1,2dithiol: Him = imidazole), a Mononuclear Manganese(III) Thiolate Possessing a Rare Manganese(III)imidazole Bond.  J. Chem. Soc., Chem. Commun., 1985, 58 60.
    84014
  4. Seela, J. L.; Folting, K.; Wang, RuJi; Huffman, J. C.; Christou, G.; Chang, HsiuRong; Hendrickson, D. N.: Manganese(III) Thiolate Chemistry: New Structural Types, Including the First MixedValence Metal Thiolate. Inorg. Chem. 1985, 24, 44546. 
    85014, 84069, 84093
  5. Lemmen, T. H.; Folting, K.; Huffman, J. C.; Caulton, K. G.: Copper Polyhydrides.  J. Am. Chem. Soc. 1985, 107, 7774.
    85066
  6. Nicholson, J. R.; Wang, RuJi; Huffman, J. C.; Christou, G.; Chang, HsiuRong; Hendrickson, D. N.: Synthesis and Structure of (PPh4)2Na[Cr3(SCH2CH2O)6] containing a Linear Chromium(III) Trimer with Terminal Thiolate and Bridging Alkoxide Linkages.  J. Chem. Soc., Chem. Commun. 1985, 178183.
    85062
  7. Ahmed, K. J.; Chisholm, M. H.; Folting, K.; Huffman, J. C.: The TungstenTungsten Triple Bond. 11. Ligand Redistribution Reactions Involving Chloride and Dimethylamide Ligands at Dimolybdenum and Ditungsten (M.tplbnd.M) Centers Induced by Added Tertiary PHosphines. Preparations and Characterizations of W2Cl2(NMe2)4(Me2PCH2PMe2), W2Cl3(NMe2)3(PMe2Ph)2, and W2Cl4(NMe2)2(PMe2Ph)2. Inorg. Chem. 1985, 24, 403944.
    83057, 83104
  8. Coffindaffer, T. W.; Rothwell, I. P.; Folting, K.; Huffman, J. C.; Streib, W. E.: Lowvalent Niobium Aryloxide Chemistry. J. Chem. Soc., Chem. Commun. 1985, 151922.
    84909
  9. Chisholm, M. H.; Heppert, J. A.; Huffman, J. C.; Streib, W. E.: Attack of Isocyanide and Carbon Monoxide on a Bridging Alkylidyne Ligand at a Ditungsten Centre. Cleavage of the CN and CO Triple Bonds with Respective Formation of Tungstenimido and oxo Groups and Concomitant Addition of the Carbon Atom to the Bridging Alkylidyne Carbon Yielding a Bridging .sigma.W1,.eta.2W2 Alkynyl Ligand.  J. Chem. Soc., Chem. Commun. 1985, 177173.
    85082
  10. Sasaki, S.; Grieco, P. A.; Huffman, J. C.; Callant, P.; Imamura, P. M.: Synthetic Studies toward Quassinoids: Anomalous Results from the MetalAmmonia Reduction of Phenanthrenone Derivatives.  J. Org. Chem. 1985, 50, 488083.
    83065, 83054, 83050
  11. Chisholm M. H.; Heppert, J. A.; Huffman, J. C.; Thorton, P.; Paramagnetic 1,3Dimetallacyclobutadienes of Tungsten(VI): 2,4Bis(trimethylsilyl)1,3dihalogeno 1,1,3,3tetrakis(trimethylsilylmethyl)1,3ditung stacyclobutadienes. J. Chem. Soc., Chem. Commun. 1985, 1466 8.
    84083
  12. Latesky, S. L.; McMullen, A. K.; Rothwell, I. P.; Huffman, J. C.: Synthetic and Mechanistic Aspects of Intramolecular Aliphatic CH Bond Activation by Ti(IV) and Zr(IV) Metal Centers.  J. Am. Chem. Soc. 1985, 107, 598187.
    83905
  13. McCarthy, J. R.; Zimmerman, M. B.; Trepanier, D. L.; LeTourneau, M. E.; Wiedeman, P. E.; Whitten, J.; Broersma, R. J.; Shea, P. J.; Wiech, N. L.; Huffman, J.C.:6,7Dihydro5[[(cis2hydroxytrans3phenoxyclclo-pentyl)amino]methyl]2methylbenzo[b]thiophen4(5H)one, a Novel .alpha.1Adrenergic Receptor Antagonist and Renal Vasodilator. J. Med. Chem. 1985, 28, 11425.
    82702
  14. Latesky, S. L.; McMullen A. K.; Niccolai, G. P.; Rothwell, I. P.; Huffman, J. C.: Intromolecular Coupling of .eta.2Iminoacyl Functions at Group 4 Metal Centers.  Organometallics. 1985, 4, 189698.
    85907
  15. Money, J. K.; Huffman, J. C.; Christou, G. C.: Vanadium (IV) Thiolate Chemistry: Preparation, Structure, and Properties of [VE(SCH2CH2S)2]2 (E = O, S). Inorg. Chem. 1985, 24, 32973302.
    83056, 84079
  16. Chisholm, M. H.; Heppert, J. A.; Hoffman, D. M.; Huffman, J. C.: The TungstenTungsten Triple Bond. 10. Ditungsten Hexapivalate.  Inorg. Chem. 1985, 24, 32147.
    84019
  17. Lawrence, S. H.; Shore, S. G.: Koetzle, T. F.: Huffman, J. C.; Wei, CYu, Bau, R.: Preparation and Xray and Neutron Diffraction Structure Determination of the Chlorotrihydroborate Ion, [BH3Cl].  Inorg. Chem. 1985, 24, 31716.
    85200
  18. Bansemer, R. L.; Huffman, J. C.; Caulton, K. G.:Synthesis and Characterization of VCl3(PMePh2)2. Inorg. Chem. 1985, 24, 30036.
    84101
  19. Smith, P. D.; Martin, J. L.; Huffman, J. C.; Bansemer, R. L.; Caulton, K. G.: Bimetallic Halides. Crystal Structure of and Ethylene Polymerization by VCl2.ZnCl2.4THF. Inorg. Chem. 1985, 24, 29973002.
    84025
  20. Huffman, J. C.; Green, M. A.; Kaiser, S. L.; Caulton, K. G.: A Lipophilic Salt of a TransitionMetal Ployhydride: KOsH3(PMe2Ph)3.  J. Am. Chem. Soc. 1985, 107, 511115.
    84104
  21. Chisholm, M. H.; Huffman, J. C.; Heppert, J. A.: 1,3Ditungstacyclobutadienes. 1. Reactions with Alkynes. Alkyne Adducts and 1,3Dimetallaallyl Derivatives. J. Am. Chem. Soc. 1985, 107, 51165136.
    84021,83103, 83087, 84031
  22. McCarthy, J. R.; Wiedeman, P. E.; Schuster, A. J.; Whitten, J. P.; Barbuch, R. J.; Huffman, J. C.: Stereospecific Syntheses of the Four Diastereomeric 2Amino5 phenoxycyclopentanols.  J. Org. Chem. 1985, 50, 3095103.
  23. Ahmed, K. J.; Chisholm, M. H.; Huffman, J. C.: A Skewed Bridging Alkyne Adduct of a d3d3 Tungsten Dimer: W2(.mu. NMe2)2(.mu.C2Me2)Cl4(py)2. Organometallics. 1985, 4, 131213.
    85005
  24. Ahmed, K. J.; Chisholm, M. H.; Huffman, J. C.: The MolybdenumMolybdenum Triple Bond. 16. Bis[(trimethylsilyl)methylidene]tetrakis(trimethylphosphine)dibromodimolybdenum (M.tplbnd.M). An Example of a Nonbridged Dinulear Bis Carbene Complex. Organometallics. 1985, 4, 116874.
    82028, 82027, 83064
  25. Marsella, M. A.; Huffman, J. C.; Folting, K.; Caulton, K. G.: Hydride Transfer from Transition Metal Hydrides to Dihapto Acyl Ligands.  Inorg. Chim. Acta., 1985, 96, 16170.
    81017
  26. Chisholm, M. H.; Folting, K.; Huffman, J. C.; Koh, J. J.: A Diphosphide Adduct of DitungstenHexaisopropoxide: Xray Crystal Structure of W2(OPr6(py)(.mu.P2). Polyhedron. 1985, 4, 89395.
    84112
  27. Chisholm, M. H.; Clark, D. L.; Huffman, J. C.: The MolybdenumMolybdenum Triple BondXVII. Syntheses, Spectroscopic and Structural Characterizations of Mo4F4(OtBu)8 and Mo2F2(OtBu)4(PMe3)2(Mo.tplbnd.Mo).  Polyhedron. 1985, 4, 120311.
    84034
  28. Chetcuti, M. J.; Chisholm, M. H.; Chiu, H. T.; Huffman, J. C.: 1,2Dimetallacyclo1,2hexyne Compounds of Molybdenum and Tungsten. Polyhedron. 1985, 4, 121318.
    84074
  29. Trimarchi, C. L.; Green, M. A.; Huffman, J. C.; Caulton, K. G.: Photoinitiated Intramolecular Hydrogen Transfer from Rhenium Polyhydrides to C8 Cyclopolyolefins.  Organometallics. 1985, 4, 51419.
    81070
  30. Green, M. A.; Welch, M. J.; Mathias, C. J.; Fox, K. A. A.; Knabb, R. M.; Huffman, J. C.: Gallium68 1,1,1Tris(5methoxysalicylaldiminomethyl)ethane: A Potential Tracer for Evaluation of Regional Myocardial Blood Flow.  J. Nucl. Med. 1985, 26, 17080.
  31. Coffindaffer, T. W.; Niccolai, G. P.; Powell, D.; Rothwell, I. P.; Huffman, J. C.: Effect of Aryloxide Ancillary Ligands on the Chemistry of Molybdenum Molybdenum and TungstenTungsten Multiple MetalMetal Bonds.  J. Am. Chem. Soc. 1985, 107, 357283
    83902
  32. Chisholm, M. H.; Folting, F.; Huffman, J. C.; Leonelli, J.; Marchant, N. S.; Smith C. A.; Taylor, L. C. E.: Tetranuclear Carbidotungsten and Nitridomolybdenum Clusters Supported by Alkoxide Ligands: W4(C)(OiPr)12(NMe) and Mo4(N)2(OiPr)12. J. Am. Chem. Soc. 1985, 107, 37224.
    82019, 85008
  33. Luetkens, M. L.; Huffman, J. C.; Sattelberger, A. P.: Tetrahydroborate Complexes of Tantalum: Synthesis, Characterization, and Reactivity of Ta(BH4)H2(PMe3)4. J. Am. Chem. Soc. 1985, 107, 33613.
    84905
  34. Chisholm, M. H.; Folting, K. F.; Huffman, J. C.; Kober, E. M.: Reactions of MetalMetal Multiple Bonds. 14. Synthesis and Characterization of TrianguloW3 and Mo2Woxo Capped Alkoxide Clusters. Comproportionation of MM Triple Bonds, .sigma.2.pi.4 and do Metaloxo Groups: M.tplbnd.M + M.tplbnd.O > M3(.mu.3O). Inorg. Chem. 1985, 24, 2415.
    83075
  35. Santure, D. J.; Huffman, J. C.; Sattelberger, A. P.: Synthesis and Properties of Ditungsten(II) Tetracarboxylates.  Inorg. Chem. 1985, 24, 3718.
    82912
  36. Hanusa, T. P.; Huffman, J. C.; Curtis, T. L.; Todd, L. J.: Synthesis of (.pi.Arene)Metallocarbaboranes Containing Ruthenium or Osmium and a (.pi.cyclohexadienyl)cobaltacarborane. Crystal Structure of 2,5,6(.eta.6C6H6)RuC2B7H11. Inorg. Chem. 1985, 24, 78792.
    82204
  37. Chisholm, M. H.; Hoffman, D. M.; Huffman, J. C.: An ImidoCapped Tungsten Cluster: W3(.mu.3NH)(OiPr)10. Inorg. Chem. 1985, 24, 7967.
    84058
  38. Latesky, S. L.; Keddington, J.; McMullen, A. K.; Rothwell, I. P.; Huffman, J. C.: Synthesis, Structure, Spectroscopic Properties, and Electrochemical Behavior of Group 4 Metal Derivatives Containing Bulky Aryloxide Ligands.  Inorg. Chem. 1985, 24, 9951001.
    82905,83937
  39. Luetkens, M. L.; Santure, D. J.; Huffman, J. C.; Sattelberger, A. P.: Synthesis and Characterization of Sevencoordinate TaX(CO)3(PMe3)3 Complexes (X = Cl, Br, I)  J. Chem. Soc., Chem. Commun. 1985, 5523.
    83930
  40. Drewes, S. E.; Drewes, M. W.; McNaught, I. J.; Huffman, J. C.: Synthesis and Configurational Study of 5Acetyl5methyl2phenyl1,3dithiane.  S. Afr. J. Chem., 1985, 38, 1216.
  41. Coffindaffer, T. W.; Rothwell, I. P.; Huffman, J. C.: Dinuclear Aryloxide Chemistry. 3. Synthesis, Structure, and Fluxional Behavior of 1,2Bis(2tertbutyl6 methylphenoxy)tetrakis(dimethylamino)dimolybdenum andditungsten (M.tplbnd.M).  Inorg. Chem. 1985, 24, 16436. 
    83938
  42. McMullen, A. K.; Rothwell, I. P.; Huffman, J. C.: Coupling of Acyl and Iminoacyl Groups on Zirconium and .sigma.2,.pi. Coordination of the Resulting Enamidolate Ligand.  J. Am. Chem. Soc. 1985, 107, 10723. 
    84916
  43. Rhodes, L. F.; Huffman, J. C.; Caulton, K. G.: Multiple MixedMetal Condensation Leading to the Trigonal Bipyramidal Hexahydride Ir2Cu3H6(MeCN)3(PMe2Ph)63+. J. Am. Chem. Soc. 1985, 107, 175960.
    84061
  44. Drewes, S. E.; Grieco, P. A.; Huffman, J. C.: A Short Synthesis of dlepiPyroangolensolide and dlPyrangolensolide: Confirmation of the Structures of Pyroangolensolide and Calodendrolide. J. Org. Chem. 1985, 50, 130911.
    84070
  45. Chisholm, M. H.; Hoffman, D. M.; Huffman, J. C.: Metal Alkoxides: Models for Metal Oxides. 8. Monocarbonyl Adducts of Ditungsten Hexaalkoxides (M.tplbnd.M) (RO = tBuO, iPrO, and tBuCH2O) and the Dimer [W2(OiPr)6(.mu.CO)]2.  Organometallics. 1985, 4, 986994.
    84006,84012
  46. Chisholm, M. H.; Folting, K.; Heppert, J. A.; Hoffman, D. M.; Huffman, J. C.: Metal Alkoxides: Models for Metal Oxides. 7. Trinuclear and Tetranuclear Alkylidyne Clusters of Tungsten Supported by Alkoxide Ligands.  J. Am. Chem. Soc. 1985, 107, 123441.
    84041,84047
  47. Chisholm, M. H.; Hoffman, D. M.; Huffman, J. C.: Reactions Involving the Triple Bond in Dimolybdenum and Ditungsten Hexaalkoxides and CC, CN and CO Triple Bonds.  Chem. Soc. Rev. 1985, 14, 6991.
  48. Chisholm, M. H.; Corning, J. F.; Folting, K.; Huffman, J. C.: Triple Bonds Between Molybdenum and Tungsten Atoms Supported by Thiolate Ligands: (RS)3M.tplbnd.M(SR)3. Polyhedron. 1985, 4, 38390.
    83046,84011
  49. Boyar, E. B.; Dobson, A.; Robinson, S. D.; Haymore, Barry L.; Huffman, J. C.: Complexes of the Platinum Metals. Part 25. Reactions of Ruthenium and Osmium Nitrosyls [MH(NO)PPh3)3] and [M(NO)2(PPh3)2] with Perfluorocarboxylic Acids: The Xray Crystal Structure determination of nitrosyl(trifluoroacetato)(trifluoroacetohydroximatoOO')bis(triphenyphosphine)osmium(II)dichloromethane (1/1).  Dalton Trans. 1985, 6219.
    82503
  50. Hessen, B.; Teuben, J. H.; Lemmen, T. H.; Huffman, J. C.; Caulton, K. G.: Cyclopentadienylvanadium(III) and vanadium(II) Methyl, Phenyl, and Borohydride Compounds.  Organometallics. 1985, 4, 9468.
    84071
  51. Latesky, S. L.; McMullen, A. K.; Niccolai, G. P.; Rothwell, I. P.; Huffman, J. C.: The Chemistry of Sterically Crowded Aryl Oxide Ligands. 3. Crystal and Molecular Structure of Mixed BenzylAryl Oxide Compound of Zirconium.  Organometallics. 1985, 4, 9028.
    82940,84926, 84906
  52. Ahmed, K. J.; Chisholm M. H.; Folting K.; Huffman, J. C.: W2Cl3(NMe2)3(PMe2Ph)2 and its Reaction with Ethyne to give (PMe2Ph)Cl2W(.mu.NMe2)(.mu..sigma.,.eta.2CHCH2)(.mu..eta.2,.sigma.CH2NMe)WCl(NMe2)(PMe2Ph): a Compound containing an Azadimetallabicyclobutane Core and a .sigma.,.pi.Vinyl Ligand.  J. Chem. Soc., Chem. Commun. 1985, 152153. 
    83057,84086

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