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Publications in 1988


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The numbers following each publication are linked to the structures reported in the publication.

1988
  1. Vincent, J. B.; Folting, K.; Huffman, J. C.; Christou, G.: Dinuclear ManganeseOxide Complexes as Models for Manganese Catalase.  Biochem. Soc. Trans. 1988, 16, 822-823.
    87178
  2. Westerberg, D. E.; Sutherland, B. R.; Huffman, J. C.; Caulton, K. G.: Synthetic and Mechanistic Features of Dinuclear Reductive Elimination Between Re2H8(PMe2Ph)4 and Several Tin(II) Reagents.  J. Am. Chem. Soc. 1988, 110, 1642-1643.
    87067
  3. Chisholm, M. H.; Hammond, C. E.; Huffman, J. C.: Tetrakisdimethylamidozirconium and its Dimethylamido Lithium Adduct: Structures of[Zr(NMe2)4]2 and Zr(NMe2)6Li2(THF)2.  Polyhedron. 1988, 7, 2515-2520.
    87230, 87234
  4. Lappas, D.; Hoffman, D. M.; Folting, K.; Huffman, J. C.: Synthesis and Structure of a Resonance Stabilized (Trimethylphosphonio)metallapropenide.  Angew. Chem. Int. Ed. Engl. 1988, 26, 587-589. 
    87813
  5. Kester, J. G.; Huffman, J. C.; Todd, L. J.: Further Synthetic Studies of B9H11NH. The Crystal Structure of 1(.eta.5C5H5)1,2CoNHB9H9.  Inorg. Chem. 1988, 27, 4528-4532. 
    86110
  6. Boyd, P. D. W.; Li, Q.; Vincent, J. B.; Folting, K.; Chang, H.R.; Streib, W. E.; Huffman, J. C.; Christou, G.; Hendrickson, D. N.: Potential Building Blocks for Molecular Ferromagnets: [Mn12O12(O2CPh)16(H2O)4] with a S = 14 Ground State. J. Am. Chem. Soc. 1988, 110, 8537-8539.
    86156
  7. Lundquist, E. G.; Folting, K.; Huffman, J. C.; Caulton, K. G.: A Single Bond Covalent Radius for IrIII: Crystal and Molecular Structure of facIr(CH3)3(PMe2Ph)3.  Polyhedron. 1988, 7, 2171-2173.
    87223
  8. Hites, R. A.; Koester, C. J.; Huffman, J. C.: The Crystal Structure of Octachlorodibenzodioxin: Experimental and Calculated.  Chemosphere, 1988, 17, 2419-2422.
    88032
  9. Magnus, P.; Matthews, I. R.; Schultz, J.; Waditschatka, R.; Huffman, J. C.: Synthesis of the Hexacyclic Indole Alkaloid (+)Kopsijasmine.  J. Organomet. Chem. 1988, 53, 5772-5776.
    85059, 85078
  10. Hazin, P. N.; Huffman, J. C.; Bruno, J. W.: Preparation, Luminescence Studies, and Solution Behaviour of a Cerium Tungsten Heterobimetallic Compound. J. Chem. Soc, Chem. Comm. 1988, 22, 1473-1474.
    87832
  11. Chisholm, M. H.; HampdenSmith, M. J.; Huffman, J. C.; Martin, J. D.; Stahl, K. A.; Moodley, K. G.: The TungstenTungsten Triple BondXVI. Bis(cyclopentadienyl) and Bis(indenyl)tetradimethylamidoditungsten (W.tplbnd.W).  Polyhedron. 1988, 7, 1991-1999. 
    87155, 88021
  12. Lundquist E. G. ; Huffman, J. C.; Folting K.; Caulton, K. G.: Mechanism of Ethylene Hydrogenation by the Molecular Hydrogen Complex [Ir(H)2(H2)(PMe2Ph)3] Characterization of Intermediates.  Angew. Chem. Int. Ed. Engl. 1988 27, 1165-1167. 
    87201
  13. Magnus, P.; Lewis, R. T.; Huffman, J. C.: Synthesis of a Remarkably Stable Bicyclo [7.3.1]diynene Esperamicin A1/Calicheamicin.gamma. System. Structural Requirements for Facile Formation of a 1,4Diyl.  J. Am. Chem. Soc. 1988, 110, 6921-6923.
    88077, 88094
  14. Vincent J. B.; Huffman J. C.; Christou, G.; Li, Q.; Nanny, M. A.; Hendrickson D. N.; Fong, R. H.; Fish, R. H.,: Modeling the Dinuclear Sites of Iron Biomolecules: Synthesis and Properties of Fe2O(OAc)2Cl2(bipy)2 and Its Use as an Alkane Activation Catalyst.  J. Am. Chem. Soc. 1988, 110, 6898-6900.
    88005
  15. Buhro, W. E.; Chisholm, M. H.; Folting, K.; Huffman, J. C.: Martin, J. D.; Streib, W. E.: Unbridged and Bridged Isomers of W2(PCy2)2(NMe2)4: Preparations, Characterizations, and Comments on Thermodynamic and Activation Parameters for the Closing of Phosphido Bridges in d3d3 Dinuclear Compounds. J. Am. Chem. Soc. 1988, 19, 6563-6565.
    87013
  16. Money, J. K.; Huffman, J. C.; Christou, G.: Metal/Sulfide/Thiolate Chemistry for an Early 3d Transition Metal: Variation of Product Identity as a Function of V:S Reaction Ratio and Structure and Redox Properties of Discrete V/S/edt Complexes. Inorg. Chem. 1988, 27, 507­514.
    85160, 86154
  17. Bergs, D. J.; Chisholm, M. H.; Folting, K.; Huffman, J. C.; Stahl, K. A.: Preparation and Characterization of the Heptachlorobis(tetrahydrofuran)ditungstate and Octachloro(tetrahydrofuran)ditungstate Anions: [Ph4P][W2C17(THF)2] and [Ph4P][W2C18(THF)].  Inorg. Chem. 1988, 27, 2950-2954.
    87032, 87057
  18. Pelati, J. E.; Huffman, J. C.; Wentworth, R. A. D.: Tetranuclear Molybdenum Compounds Containing a .mu.4Disulfide Linkage.  Inorg. Chem. 1988, 27, 2194-2196.
    85202
  19. Huffman, J. C.; Moloy, K. G.; Caulton, K. G.: A Titanium Alkoxide (Pinacolate) Complex Incorporating a 10Membered Ring.  Inorg. Chem. 1988, 27, 2190-2192.
    8016
  20. Chisholm, M. H.; Clark, D. L.; Errington, R. J.; Folting, K. and Huffman, J. C.: Tetranuclear HalideAlkoxide Clusters of Molybdenum Formed by the Coupling of MM TripleBonded Dinuclear Compounds. Synthesis, Characterization, and Molecular Structures of Mo4F2(OiPr)10, Mo4X3(OiPr)9, and Mo4X4(Oi Pr)8 (X=Cl, Br, I). Inorg. Chem. 1988, 27, 2071-2084.
    81021, 81063, 83038, 85035
  21. Blatchford, T. P., Chisholm, M. H.; Huffman J. C.: Reactions of MetalMetal Multiple Bonds. 15. Reactions of M2(OR)6(M.tplbnd.M) Compounds (M = Mo, W) with 9,10Phenanthrenequinone and Tetrachloro1,2benzoquinone.  Inorg. Chem. 1988, 27, 2059-2070.
    82081, 83122, 83121, 82084
  22. Peet, N. P.; Sunder, S.; Barbuch, R. J.; Whalon, M. R.; Huffman, J. C. J.: Reinvestigation of the Condensation of 2Hydrazinobenzothiazole with Ethyl Acetoacetate.  Heterocyclic Chem. 1988, 25, 543-547.
    86707
  23. Green, M. A.; Huffman, J. C. J.: The Molecular Structure of Indium Oxine.  J. Nucl. Med. 1988, 29, 417-420. 
    86821
  24. Chisholm, M. H.; HampdenSmith, M. J.; Huffman, J. C.; Moodley, K. G.: Diallyland Bis(2methylallyl)tetrakis(dimethylamido)ditungsten: W2(.mu..eta.3C3H5)2(NMe2)4 and W2(.eta.1C4H7)2(NMe2)4 (M.tplbnd.M). Comments on LigandMetal .pi.Interactions at (W.tplbnd.W)6+ Centers. J. Am. Chem. Soc. 1988, 110, 4070-4071. 
    88058
  25. Chisholm, M. H.; Eichhorn, B. W.; Folting, K.; Huffman, J. C.: The TungstenTungsten Triple Bond. XV. Synthesis, Structure and Reactivity of 1,2W2[CH(SiMe3)2]2(NMe2)4: the Remarkable Inertness of a Stericallyencumbered TungstenAmido Complex.  Inorg. Chim. Acta, 1988, 144, 193-199.
    87039
  26. Chisholm, M. H.; Hammond, C. E.; Huffman, J. C.: Mo(NMe2)6Li2(THF)2. Polyhedron. 1988, 7, 399-400.
    87151
  27. Christmas, C.; Vincent, J. B.; Chang, H. R.; Huffman, J. C.; Christou, G.; Hendrickson, D. N.: Nonanuclear OxideBridged Manganese Complex. Preparation, Structure, and Magnetic Properties of [Mn9O4(O2CPh)8(sal)4(salH)2(pyr)4] (salH2 = Salicylic Acid; pyr = Pyridine).  J. Am. Chem. Soc. 1988, 110, 823-830.
    86109
  28. Collison, D.; Mabbs, F. E.; Temperley, J.; Christou, G,; Huffman, J. C.: Crystal and Molecular Structure of Bis(tetraphenylphosphonium) Bis(1,2dicyanoethylene1,2dithiolato)oxovanadate(IV). Its SingleCrystal Electron Spin Resonance as a Pure Compound and Diluted in the Isomorphous Molybdenum(IV) Compound. J. Am. Chem. Soc. 1988, 309-314.
    85061
  29. Kerschner, J. L.; Rothwell, I. P.; Huffman, J. C.; Streib, W. E.: The Conversion of Chelated .eta.6Arene to .sigma.Aryl Coordination at Tungsten Metal Centers.  Organometallics. 1988, 7, 1871-1873.
    87917, 87918
  30. Yang, D. C.; Dragisich, V.; Wulff, W. D.; Huffman, J. C.: Insertion Reactions of ChromiumCarbene Complexes with Organic Nitriles and a Diastereoselective Alkylation of a Resulting IminoCarbene Complex. J. Am. Chem. Soc. 1988, 110, 307-309.
    84937, 87801, 85805
  31. Chisholm, M. H.; Huffman, J. C.; Marchant N. S.: A Study of the Reaction Between Mo2(OCH2CMe3)6(.mu..eta.1,.eta.2NCNR2) Compounds (R=Me and Et) and 2Butyne. Polyhedron. 1988, 7, 919-930.
    85069, 84064
  32. Chisholm, M. H.; Conroy, B. K.; Clark, D. L.; Huffman, J. C.: Metal Alkoxides: Models for Metal Oxides. XIII. NMR Spectroscopic and Theoretical Investigations into the Reduction of Alkynes Bonded to Hexaalkoxides of Dimolybdenum and Ditungsten.  Polyhedron. 1988, 7, 903-918.
  33. Bashkin, J. S.; Schake, A. R.; Vincent, J. B.; Chang, H. R.; Li, Qiaoying; Huffman, J. C.; Christou, G.; Hendrickson, D. N.: Mixed Valence Manganese(II,III) and (III,IV) Dinuclear Complexes: Preparation, Structure, Magnetochemistry, and E.S.R. Spectra of Mn2(biphen)2(biphenH)(bpy)2 and Mn2O2C12(OAc)(bpy)2 (biphenH2 = 2,2' biphenol, bpy = 2,2' bipyridine).  J. Chem. Soc., Chem. Comm., 1988, 700-702.
    87053, 87038
  34. Chesnut, R. W.; Steffey, B. D.; Rothwell, I. P.; Huffman, J. C.: Cyclotantalation of 2,6diphenylphenoxide; Xray crystal structure of Ta(OC6H3PhC6H4)(OAr2,6Ph2)2Me. Polyhedron. 1988, 7, 753-756.
    87910
  35. Williams, R. A.; Hanusa, T. P.; Huffman, J. C.: Solid State Structure of Bis(pentamethylcyclopentadienyl)barium, (Me5C5)2Ba; the First XRay Crystal Structure of an Organobarium Complex. J. Chem. Soc., Chem. Comm. 1988, 1045-1047.
    87837
  36. Larson, E. J.; Van Dort, P. C.; Lakanen, J. R.; O'Neill, D. W.; Pederson, L. M.; McCandless, J. J.; Silver, M. E.; Russo, S. O; Huffman, J. C.: Factors Determining Allyl Hapticity in EarlyTransitionMetal Allyl Complexes: Synthesis, Structure, and Dynamics of Cp2(.eta.31,2,3 Me3allyl)ZrBr and Cp2(.eta.11,1,2Me3allyl)ZrBr.  Organometallics. 1988, 7, 1183-1187.
    86812, 86811
  37. Galante, J. M.; Bruno, J. W.; Hazin, P. N.; Folting, K.; Huffman, J. C.: Kinetic and Mechanistic Studie on the Formation and Reactions of EarlyTransitionMetalKetene Complexes. Organometallics.1988, 7, 1066-1073.
    87827
  38. Chisholm, M. H.; Folting, K.; Huffman, J. C.; Klang, J. A.: W3(OiPr)9(Cl)2(.mu.3CMe). An Unexpected Mode of .mu.3Ethylidyne Bonding and Dynamic Solution Behavior. Organometallics. 1988, 7, 1033-1036.
    87102
  39. Van Der Sluys, W. G.; Burns, C. J.; Huffman, J. C.,; Sattelberger, A. P.:Uranium Alkoxide Chemistry. 1. Synthesis and the Novel Dimeric Structure of the First Homoleptic Uranium(III) Aryloxide Complex. J. Am. Chem. Soc. 1988, 110, 5924-5925.
    87834
  40. Folting, K.; Huffman, J. C.Mahoney, W.; Stryker, J. M.; Caulton, K. G.: Structure of Chlorotris(triphenylphosphine)copper(I) Tetrahydrofuran(1/3).  Acta Cryst., 1987, C43, 1490-1492.
    86159
  41. Chisholm, M. H.; Folting, K.; Pasterczyk, J. W: A Phosphido-Capped Tritungsten Alkoxide Cluster: W3(?3-P)(?-OCH2-t-Bu)3(OCH2-t-Bu)6 and Speculation upon the Existence of a Reactive (t-BuCH2O)3W=P Intermediate. Inorg. Chem. 1988, 27, 3057-3058.
    88022
  42. Chisholm, M. H.; Folting, K.; Hammond, C. E.; Hampden-Smith, M. H. A New Class of Homoleptic 12-Electron Molybdenum and Tungsten Alkoxide Clusters of Formula [M4(OR)12].  J. Am. Chem. Soc. 1988, 110, 3314-3315.
    88009
  43. Geerts, R. L.; Huffman, J. C.; Westerberg, D. E.; Folting, K.; Caulton, K. G.: Zinc-Containing Heterometallic Hydride Compounds: Observation of Terminal and Bridging ZnN(SiMe3)2 Groups. New. J. Chem., 1988, 12, 455-465.
    85149, 85112, 85111
  44. Hazin, P. N.; Lakshminarayan, C.; Brinen, L. S.; Knee, J. L.; Bruno, J. W.; Streib, W. E.; Folting, K.: Luminescence Spectra and Lifetimes of Cerium(III) Compounds as Indicators of Solution Behavior and Radiative Efficiency. Inorg. Chem. 1988, 27, 1393-1400.
    87812

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