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Publications in 1991


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The numbers following each publication are linked to the structures reported in the publication.

1991
  1. Hampden-Smith, M.J., Wark, T.A., Rheingold, A.L., Huffman, J. C.: Solid state and solution structural investigation of homoleptic tin(IV) alkoxide compounds. Part I. Sn(O-t-Bu)4 and [Sn(O-i­Pr)4 · HO-i-Pr]2.Can. J. chem. 1991, 69, 121-129.
    88907
  2. McGeary, M.J.; Folting, K.; Streib, W. E.; Huffman, J. C.; Caulton, K.G.: Oligomerization and Structural Variation of Alkali Metal Silyloxides.Polyhedron. 1991, 10, 2699-2709.
    89172, 89192, 89273
  3. Chisholm, M. H.; Parkin, I. P.; Huffman, J. C.; Lobkovsky, E. M.; Folting, K.: The Preparation and Characterization of M2(OEPh3)2(NMe2)4, Where M=Mo and W and E=C and Si. The X-ray Crystal Structures of Gauche-W2(OCPh3)2(NMe2)4, Anti-Mo2(OCPh3)2(NMe2)4, and Anti-W2(OSiPh3)2(NMe2)4. Polyhedron. 1991, 10, 2839-2846.
    90218, 90219, 90366
  4. Hampden-Smith, M. J.; Garvey, J.; Lei, D.; Huffman, J. C.: Chemical Vapor Deposition of Binary Metal Germanides in Thin Film Structures and Phase Stability. Mater. Res. Soc. Symp. Proc. 1991, 187.
  5. Cayton, R. H.; Chisholm, M. H.; Huffman, J. C.; Lobkovsky, E. B.: Mo-Mo Quadruple Bonds Bridged by 1,8-Naphthyridinyl-2,7-Dioxide: an Insight into the Nature of a Parallel-Linked Stiff-Chain Polymer: [~MnM~~~MnM]x. Angew. Chem. Int. Ed. Engl. 1991, 30, 862-864.
    90294
  6. Chisholm, M. H.; Huffman, J. C.; Lucas, E. A.; Lobkovsky, E. B.: Addition of 1,3-Butadiene to a Metal-Metal Triple Bond. Preparation and Structure of W2(OCH2-t-Bu)6(py)(C4H6). Organometallics. 1991, 10, 3424-3425.
    91122
  7. Chacon, S. T.; Chisholm, M. H.; Folting, K.; Huffman, J. C.; Hampden-Smith, M. J.: Allene Adducts of Ditungsten Hexaalkoxides. Three Modes of Allene Coordination to Dinuclear Centers as Seen in the Structures of W2(O-t-Bu)6(C3H4), W2(O-t-Bu)6(C3H4)2, and W2(O-t-Bu)6(C3H4)(CO)2. Organometallics. 1991, 10, 3722-3735.
    88167, 89021, 88214
  8. Hauger, B. E.; Vance, P. J.; Prins, T. J.; Wemple, M. E.; Kort, D. A.; Silver, M. E.; Huffman, J. C.: Hafnium halide compounds of methyl substituted allyl ligands. Synthesis, crystal structure and dynamics of (.eta.5-C5Me5)(.eta.3-1,2,3-Me3allyl)HfBr2 and (.eta.5-C5Me5)(.eta.3-1,2,3-Me3allyl)HfBr2. Inorg. Chim. Acta. 1991, 187, 91-97.
    89923, 89903
  9. Lei, D.; Hampden-Smith M. J.; Garvey, J. W.; Huffman, J. C.: The Chemistry of Transition Metal-Germanium Compounds. Part 2. Synthesis, Characterization, Structure and Reactivity of Transition-metal Carbonyl-substituted Germacyclopent-3-enes. Dalton Trans. 1991, 2449-2457.
    89925, 89916, 89919.
  10. Perlepes, S. P.; Huffman. J. C.; Christou, G.: Preparation and Characterization of [Mn11O10Cl2(OAc)11(bpy)2(MeCN)2(H2O)2](ClO4)2 · 8MeCN, a Mixed-valence Manganese(III/IV) Aggregate with Rare Undecanuclearity (bpy = 2,2'-bipyridyl). J. Chem. Soc., Chem. Commun. 1991, 1657-1659.
    89276
  11. Eichhorn, B. W.; Kerby, M. C.; Ahmed, K. J.; Huffman, J. C.: Reactions of Mo2(O2CMe)4 with Amines and Diamines: A Structural and Thermal Study of Stepwise Acetate Displacement and Hydrogen Bonding. Polyhedron. 1991, 10, 2573-2585.
    89915, 89928
  12. Perlepes, S. P.; Huffman, J. C.; Christou, G.:Preparation and Characterization of Triply-Bridged Dinuclear Copper(II) Complexes Containing the [Cu2(.mu.-OH)(.mu.-X)(.mu.-OAc)]+ Core (X = Cl, Br), and the Crystal Structure of [Cu2(OH)Cl(OAc)(bpy)2](ClO4) · H2O. Polyhedron. 1991, 10, 2301-2308.
    90178
  13. Nicholson, J. R.; Christou, G.; Wang, R. J.; Huffman, J. C.; Chang, H. R.; Hendrickson, D. N.: A Linear Trinuclear Chromium(III) Complex with Mixed Thiolate/Alkoxide Ligation: Preparation and Properties of (PPh4)2(Na)[Cr3(SCH2CH2O)6]. Polyhedron. 1991, 10, 2255-2263.
    85062
  14. Jones, E. L.; Reynolds, J. G.; Huffman, J. C.; Christou, G.: Deoxygenation of Oxovanadium(IV) Complexes Under Mild Conditions: Synthesis and Structural Characterization of cis-Dihalobis(dialkyldithiocarbamato)vanadium(IV). Polyhedron. 1991, 10, 1817-1825.
    90019, 90056
  15. Cayton, R. H.; Chisholm, M. H.; Huffman, J. C.; Lobkovsky, Emil B.: Metal-Metal Multiple Bonds in Ordered Assemblies. 1. Tetranuclear Molybdenum and Tungsten Carboxylates Involving Covalently Linked M-M Quadruple Bonds. Molecular Models for Subunits of One-Dimensional Stiff-Chain Polymers. J. Am. Chem. Soc. 1991, 23, 8709-8723.
    90294
  16. Chisholm, M. H.; Lucas, E. A.; Sousa, A. C.; Huffman, J. C.; Folting, K.; Lobkovsky, E.; Streib, W. E.: Reduction of .alpha.,.beta.-Unsaturated Ketones and Aldehydes by Tungsten-Tungsten Triple Bonds: Formation of 1,2 and 1,4 Adducts as opposed to C=O Cleavage. J. Chem. Soc., Chem. Commun. 1991, 847-849.
    90239, 90322, 90239, 90200
  17. Schake, A. R.; Schmitt, E. A.; Conti, Andrew J.; Streib, W. E.; Huffman, J. C.; Hendrickson, D. N.; Christou, G.: Preparation and Properties of Mononuclear and Ferromagnetically Coupled Dinuclear Manganese Complexes with 2,2'-Biphenoxide. Inorg. Chem. 1991, 30, 3192-3199.
    87148, 87038
  18. Chacon, S. T.; Chisholm, M. H.; Folting, K.; Hampden-Smith, M. J.; Huffman, J. C.: Cyclopentoxyditungsten Compounds and Crystal and Molecular Structures and Dynamic Solution Behavior of W2(.mu.-H)(O-c-C5H9)7(HNME2). Inorg. Chem. 1991, 30, 3122-3125.
    88037
  19. Chisholm, M. H.; Huffman, J. C. ; Wesemann, J. L.: Synthesis and X-ray Crystal Structures of [Me2NH2]+[Al(OSiMe3)4]- and Al2(OSiMe3)6. Polyhedron. 1991, 10, 1367-1372.
    90055, 90071
  20. Chisholm, M. H.; Parkin, I. P.; Huffman, J. C.: The Synthesis, Characterization and X-ray Structure of ANTI-W2(GePh3)2(NMe2)4. Polyhedron. 1991, 10, 1215-1219.
    90326
  21. Blackman, A. G.; Huffman, J. C.; Lobkovsky, E.; Christou, G.: Towards Functional Models of the Photosynthetic Water Oxidation Centre: Synthesis and Structure of the Asymmetric Complex [Mn2O(O2CMe)2(bpy)2(H2O)(S2O8)] · H2O(bpy = 2.2'-bipyridine), containing Coordinated H2O and S2O82-. J. Chem. Soc., Chem. Commun. 1991, 989-990.
    90387
  22. Vaartstra, B. A.; Huffman, J. C.; Streib, W. E.; Caulton, K. G.: Incorporation of Barium for the Synthesis of Heterometallic Alkoxides: Synthesis and Structures of [BaZr2(OiPr)10]2 and {BaZr2(OiPr)9}2. Inorg. Chem. 1991, 30, 3068-3072. 89214,
    89269
  23. Fryzuk, M. D.; Ng, J. D.; Rettig, S. J.; Huffman, J. C.; Jonas, K.: Nature of the Catalytically Inactive Cobalt Hydride Formed upon Hydrogenation of Aromatic Substrates Structure and Characterization of the Binuclear Cobalt Hydride [{Pri2P(CH2)3PPri2}Co]2(H)(.mu.-H)3. Inorg. Chem. 1991, 30, 2437-2441.
  24. Rauscher, D. J.; Thaler, E. G.; Huffman, J. C.; Caulton, K. G.: Acidolysis of [MeC(CH2PPh2)3]Rh(CH3)n Compounds: Controlled Creation of Unsaturation. Organometallics. 1991, 10, 2209-2216.
    90130
  25. Chisholm, M. H.; Cook, C. M.; Huffman, J. C.; Streib, W. E.,: Hexakis(tert-butyldimethylsiloxy)ditungsten and Its Reaction with Ethyne. Hydrogen Atom Transfer Reactions involving Bridging Ethynyl, Ethyne, Vinyl and Ethylidyne Ligands. Crystal Structures of [W2(OSiButMe2)6], [W2(OSiButMe2)6- (.mu.-C2H2)(C5H5N)] and [W2(OSiButMe2)5(.mu.-CCH)]. Dalton Trans. 1991, 929-938.
    90003, 90020, 90046
  26. Huggins, B. A.; Ellis, P. D.; Gradeff, P. S.; Vaartstra, B. A.; Yunlu, K.; Huffman, J. C.; Caulton, K. G.: Nature of the Phase Change in Solid Ce2(OiPr)8(iPrOH)2, As Determined by Variable-Temperature X-ray Diffraction and 2H NMR Spectroscopy. Inorg. Chem. 1991, 30, 1720-1722.
    89157
  27. Prins, T. J.; Hauger, B. E.; Vance, P. J.; Wemple, M. E.; Kort, D. A.; O'Brien, J. P.; Silver, M. E.; Huffman, J. C.: Cyclopentadienyl(allyl)(butadiene)hafnium Compounds. Synthesis, Crystal Structure, and Dynamics of Cyclopentadienyl(1,2,3,-trimethylallyl)(1,2-dimethylbutadiene)-hafnium and Cyclopentadienyl(1,1,2-trimethyallyl)-(2,3-dimethylbutadiene)hafnium. Organometallics. 1991, 10, 979-985.
    89920
  28. Vance, P. J.; Prins, T. J.; Hauger, B. E.; Silver, M. E.; Wemple, M. E.; Pederson, L. M.; Kort, D. A. Kennisto, M. R.; Geerligs, S. J.; Kelly, R. S.; McCandless, J. J.; Huffman, J. C.; Peters, D. G.: Effect of Allyl Methyl Substituents on the Preparation, Dynamics, and Reactivity of Zirconium Complexes (.eta.5-C5Me5)(allyl)ZrX2 Complexes (X = Cl, Br): Structure of (.eta.5-C5Me5)(C3H5)ZrCl2 and (.eta.5-C5Me5)(1,2-Me2(butadiene))(.eta.2-CH2PPh2)Zr. Dynamics of (.eta.5-C5Me5)(2,3-Me2(butadiene))(.eta.2-CH2PPh2)Zr. Organometallics. 1991, 10, 917-924.
    89930, 89905
  29. Perlepes, S. P.; Blackman, A. G.; Huffman, J. C.; Christou, G.: Complete Carboxylate Removal from Mn12O12(OAc)16(H2O)4.2HOAc.4H2O with Me3SiCl: Synthesis and Caracterization of Polymeric [MnCl3(bpy)].eta. and an Improved Synthesis of (NEt4)2MnCl5. Inorg. Chem. 1991, 30, l665-l668.
    89281, 89481
  30. Bryan, J. C.; Wheeler, D. R.; Clark D. L.; Huffman, J. C.; Sattelberger, A. P.: The First Homoleptic Alkoxide Dimers of Rhenium(V) and Tungsten(V). Stereochemical Consequences of Metal-Metal Bonding in Edge-Shared Bioctahedra. J. Am. Chem. Soc. 1991, 113, 3184-3186.
    90605, 90602
  31. McCusker, J. K.; Vincent, J. B.; Schmitt, E. A.; Mino, M. L.; Shin, K.; Coggin, D. K.; Hagen, P. M.; Huffman, J. C.; Christou, G. C.; Hendrickson, D. N.: Molecular Spin Frustration in the [Fe4O2]8+ Core: Synthesis, Structure, and Magnetochemistry of [Fe4O2(O2CR)7(bpy)2](ClO4) (R = Me,Ph).J. Am. Chem. Soc. 1991, 113, 3012-3021.
    88019
  32. Perlepes, S. P.; Huffman, J. C.; Matonic, J. H.; Dunbar, K. R.; Christou, G.: Binding of 2,2'-Bipyridine to the Dirhodium(II) Tetraacetate Core: Unusual Structural Features and Biological Relevance of the Product Rh2(OAc)4(bpy). J. Am. Chem. Soc. 1991, 113, 2770-2771.
    90180
  33. Chisholm, M. H.; Folting, K.; Huffman, J. C.; Lucas, E. A.: Cycloalkyne Ligands Formed by the Coupling of Polymethylene-Bridged Alkylidynes: LnM.=.C(CH2)nC.=MLn ? L2nM2[.mu.-C2(CH2)n]. Organometallics. 1991, 10, 535-537.
    90080, 90117
  34. Vaartstra, B. A.; Huffman, J. C.; Streib, W. E.; Caulton, K. G.: Syntheses and Structures of a Series of Very Low Coordinate Barium Compounds: Ba[N(SiMe3)2]2(THF)2,{Ba[N(SiMe3)2]2(THF)}2, and {Ba[N(SiMe3)2]2}2. Inorg. Chem. 1991, 30, 121-125.
    90168, 89190, 90159
  35. Cayton, R. H.; Chisholm, M. H.; Davidson, E. R.; DiStasi, V. F.; Du, P.; Huffman. J. C.: Crystal and Molecular Structure of Al2(O-t-Bu)6. Comments on the Extent of M-O .pi. Bonding in Group 6 and Group 13 Alkoxides. Inorg. Chem. 1991, 30, 1020-l024.
    89170
  36. Heinrich, D. D.; Folting K.; Huffman, J. C.; Reynolds, J. G.; Christou, G.: Preparation and Properties of Mononuclear Vanadium Thiolates: Structural Characterization of the [V(SBut)4]0,- Pair and C-S Bond Cleavage in V(SBut)4 in the Gas Phase. Inorg. Chem. 1991, 30, 300-305.
    88050, 89008
  37. Budzichowski, T. A.; Chacon, S. T.; Chisholm, M. H.; Feher, F. J. and Streib, W. E.: Dimolybdenum and Ditungsten Derivatives of the Trisilanol [(c-C6H11)7Si7O9(OH)3]: [(c-C6H11)7Si7O12]2Mo2 (M/M) and [(c-C6H11)7Si7O12]2W2(µ-H)(O-t-Bu). J. Am. Chem. Soc. 1991, 113, 689-691.
    90249
  38. Yunlu, K.; Gradeff, P. S.; Edelstein, N.; Kot, W.; Shalimoff, G.; Streib, W. E.; Vaartstra, B. A. and Caulton, K. G.: Photoreduction of Cerium(IV) in Ce2(OiPr)8(iPrOH)2. Characterization and Structure of Ce4O(OiPr)13(iPrOH). Inorg. Chem. 1991, 30, 2317-2321.
    90022
  39. Lunder, D. M.; Lobkovsky, E. B.; Streib, W. E. and Caulton, K. G.: Alkoxide B-Donation to Iridium (III). J. Am. Chem. Soc. 1991, 113, 1837-1838.
    90203
  40. Chisholm, M. H.; Drake, S. R.; Nainii, A. A. and Streib, W. E.: Synthesis and X-Ray Crystal Structures of the One-Dimensional Ribbon Chains [MOBut.ButOH]4 and the Cubane Species [MOBut]4 (M = K and Rb). Polyhedron. 1991, 10, 337-345.
    90100, 90041, 90146, 90157
  41. Caulton, K. G.; Chisholm, M. H.; Streib, W. E. and Xue, Z.: Direct Observation of "-Hydrogen Transfer from Alkyl to Alkylidyne Ligands in (Me3CCH2)3W/CSiMe3. Kinetic and Mechanistic Studies of Alkyl-Alkylidyne Exchange. J. Am. Chem. Soc. 1991, 113, 6082-6090.
    90295
  42. Chisholm, M. H.; Drake, S. R.; Naiini, A. A. and Streib, W. E.: The Synthesis and Characterization of Volatile Lithium Alkoxides and the Single Crystal X-ray Structure of [LiOCMe2Ph]6. Polyhedron. 1991, 10, 805-810.
    90181
  43. Casas, J. M.; Chisholm, M. H.; Sicilia, M. V. and Streib, W. E.: Imino-Ether Complexes of Platinum: cis-[PtCl2(NH=C-(OR)Me)2] and [PtCl4(NH=C(OR)Me)2], Where R=Me,Et and Pri. Preparation, Characterization and X-Ray Structure for [PtCl2(NH=C(OPri)Me)2]2. Polyhedron. 1991, 10, 1573-1578.
    90198
  44. Coan, P. S.; Streib, W. E. and Caulton, K. G.: A Triangular Heterometallic Siloxide Containing Barium. Inorg. Chem. 1991, 30, 5019-5023.
    90348
  45. Fuentes, G. R.; Coan, P. S.; Streib, W. E. and Caulton, K. G.: Eta-6 Bonding of Benzene to Potassium in [(C6H6)KOSiMe2Ph]4. Polyhedron. 1991, 10, 2371-2375.
    91082
  46. Wang, S.; Huffman, J. C.; Folting, K.; Streib, W. E.; Lobkovsky, E. B. and Christou, G.: (NBu4)[Mn4O2(H2O)(O2CPh)9], a Butterfly Complex with Bound H2O, and Its Use to Prepare Octanuclear and Undecanuclear Metal Complexes. Angew. Chem. Int. Ed. Engl. 1991, 30, 1672-1674.
    90347, 91135, 91049
  47. Folting, K.; Streib, W. E.; Caulton, K. G.; Poncelet, O. and Hubert-Pfalzgraf, L. G.: Characterization of Aluminum Isopropoxide and Aluminosiloxanes. Polyhedron. 1991, 10, 1639-1646.
    90023
  48. Libby, E.; McCusker, J. K.; Schmitt, E. A.; Folting, K.; Hendrickson, D. N and Christou, G.: Preparation and Properties of Models for the Photosynthetic Water Oxidation Center: Spin Frustration in the [Mn4O2(O2CR)7(pic)2]- anion. Inorg. Chem. 1991, 30, 3486-3495.
    88149
  49. Bianchini, C.; Caulton, K. G.; Chardon, C.; Eisenstein, O.; Folting, K.; Johnson, T. J.; Meli, A.; Peruzzini, M.; Rauscher, D. J.; Streib, W. E. and Vizza, F.: An 04-Benzene Species Mediates Acetylene Cyclo-trimerization. J. Am. Chem. Soc. 1991, 113, 5127-5129.
    90214, 90354
  50. Wang, S.; Folting, K.; Streib, W. E.; Schmitt, E. A.; McCusker, J. K.; Hendrickson, D. N. and Christou, G.: Chloride-Induced Conversion of [Mn4O2(OAc)6(py)2(dbm)2] to [Mn4O3Cl(OAc)3(dbm)3] : Potential Relevance to Photosynthetic Water Oxidation. Angew. Chem. Int. Ed. Engl. 1991, 30, 305-306.
    89204, 89203
  51. McGeary, M. J.; Coan, P. S.; Folting, K.; Streib, W. E. and Caulton, K. G.: Yttrium and Lanthanum Silyloxide Complexes.Inorg. Chem. 1991, 30, 1723-1735.
    89014, 89064, 89072, 89120, 89166
  52. Caulton, K. G.; Chisholm, M. H.; Drake, S.R.; Folting, K.: Synthesis and Molecular Structure of a Mononuclear Barium Aryloxide-Ethanolamine Complex, Ba(2,6-But2C6H3O)2(HOCH2CH2NMe2)4 · 2C7H8, Exhibiting Extensive Hydrogen Bonding. Inorg. Chem. 1991, 30, 1500-1503.
    90188
  53. Chisholm, M. H.; Parkin, I. P. ; Folting, K.; Lobkovsky, E. B.; Streib, W. E.: Diolates of Dimolybdenum and Ditungsten (M/M) with Seven-, Eight-, and Nine-membered Rings. J. Chem. Soc., Chem. Commun. 1991, 1673-1675.
    91026, 91041, 91142, 91176
  54. Chisholm, M. H.; Parkin, I. P.; Streib, W. E.; Folting, K.: Mixed Alkoxide-Anilide d3-d3 Dimers of Molybdenum and Tungsten. The X-Ray Crystal Structures of M2(OBut)4(HNPh)2(H2NPh)2 (M = Mo, W). Polyhedron. 1991, 10, 2309-2316.
    90232, 90292

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