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Publications in 1995


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The numbers following each publication are linked to the structures reported in the publication.

1995
  1. Johnson, T. J.; Folting, K.; Streib, W. E.; Martin, J. D.; Huffman, J. C.; Jackson, S. A.; Eisenstein, O.; Caulton, K. G.: pi-Stabilized, yet Reactive, Half-Sandwich Cp*Ru(PR3)X Compounds: Synthesis, Structure, and Bonding. Inorg. Chem. 1995, 34, 488-499.
    91234, 91294, 91339, 92020, 91339
  2. Budzichowski, T. A.; Chisholm, M. H.; Tiedtke, D. B.; Huffman, J. C.; Streib, W. E.: Dicarbonyl and Tricarbonyl Adducts of (W=W)6+-Containing Complexes. Preparation and Structures of W2(OCMe2CF3)6(CO)2 and W2(OCMe(CF3)2)4(NMe2)2(CO)3. Organometallics. 1995, 14, 2318-2324.
    93251, 94017
  3. Blau, R. J.; Chisholm, M. H.; Eichhorn, B. W.; Huffman, J. C.; Kramer, K. S.; Lobkovsky, E. B.; and Streib, W. E.: Tungsten-Carbon, Carbon-Carbon, and Carbon-Hydrogen Bond Activations in the Chemistry of 1,2-W2R2(OR')4 (W=W) Complexes. 4. Phosphine- and Amine-Promoted Ligand Migrations and alpha-CH Activations in the Formation of Alkylidynehydridoditungsten Compounds. Organometallics. 1995, 14, 1855-1869.
    85139, 86136, 87007, 90190, 90307, 91005
  4. Shaw, S. L.; Morris, R. J.; Huffman, J. C.: Monoindenyl halides of zirconium and hafnium. The preparation of [(eta5-C9H7)ZrCl3]n and [(eta5-C9H7)HfCl2(-Cl)]2 and the crystal structure of [(eta5-C9H7)HfCl2(-Cl)]2. J. Organomet. Chem. 1995, 489, C4-C6.
    93912
  5. Budzichowski, T. A.; Chisholm, M. H.; Folting, K.; Huffman, J. C.; Streib. W. E.: Dimetal Hepta- and Octaalkoxide Anions of Molybdenum and Tungsten, M2(OR)7- and M2(OR)82-(M=M). Preparation, Structures, Oxidation, and a Study of the Thermal Decomposition of W2(OR)7- to Give W2(H)(O)(OR)6- Where R =tBu and iPr. J. Am. Chem. Soc. 1995, 117, 7428-7440.
    92093, 93021, 94117, 94127
  6. Laurent, F.; Huffman, J. C.; Folting, K.; Caulton, K. G.: Synthesis and Characterization of Volatile Sodium Yttrium Fluoroalkoxides. Structure of Na3Y(OCH(CF3)2)6(THF)3 and Na2Y(OCMe(CF3)2)5(THF)3. Inorg. Chem. 1995, 34, 3980-3985.
    93056, 93080
  7. Halcrow, M. A.; Huffman, J. C.; Christou, G.: A Nickel(II) Azide Cubane: Characterization of the Magnetic Exchange Interactions Mediated by a Triply Bridging Azide Group Bound End-On. Angew. Chem. Int. Ed. Engl. 1995, 34, 889-891.
    94301
  8. Scheer, M.; Becker, U.; Chisholm, M. H.; Huffman, J. C.; Lemoigno, F.; Eisenstein, O.: [Cp"Co(P4){(Cp"Co)2(µ-CO)}] (Cp"=h5-C5H3tBu2): A Complex with a P4 Unit on the Way to a P1 and a P3 Ligand. Inorg. Chem. 1995, 34, 3117-3119.
    93086
  9. Wermer, J. R.; Hollander, O.; Huffman, J. C.; Krause Bauer, J. A.; Dou, D.; Hsu, L-Y.; Leussing, D. L.; Shore, S. G.: Iodide Complexes of Decaborane(14) and 2,4-Diiododecaborane(14). The X-ray Crystal Structure of [P(C6H5)3CH3][2,4-I2B10H12I]. Inorg. Chem. 1995, 34, 3065-3071.
  10. Teff, D. J.; Huffman, J. C.; Caulton, K. G.: Influence of Lead(II) Lone Pairs on the Serpentine Structures for Heterometallic Alkoxides. Inorg. Chem. 1995, 34, 2491-2492.
    94116, 94288
  11. Samuels, J. A.; Folting, K.; Huffman, J. C.; Caulton, K. G.: Structure/Volatility Correlation of Sodium and Zirconium Fluoroalkoxides. Chem. Mater. 1995, 7, 929-935.
    93261, 93281
  12. Zwanziger, J. W.; Tagg, S. L.; Huffman, J. C.: Broken Bond-Bending Constraints and Glass Formation in the Oxides. Science. 1995, 268, 1510-1511.
    93271
  13. Perlepes, S. P.; Huffman, J. C., Christou, G. Paschalidou, S.: Dinuclear Copper(II) Complexes with the New [Cu2(µ-OR)(µ-OAc)2]- (R = Alkyl) Core: Preparation and Characterization of [Cu2(OR)(OAc)2(bpy)2]+ (R = Me, Et, Prn) Salts. Polyhedron. 1995, 14, 1073-1081.
    89093, 90047
  14. Halcrow, M. A.; Sun, J. S.; Huffman, J. C.; Christou, G.: Structural and Magnetic Properties of [Ni4(mu3-OMe)4(dbm)4(MeOH)4] and [Ni4(eta,mu3-N3)4(dbm)4(EtOH)4]. Magnetostructural Correlations for [Ni4X4]4+ Cubane Complexes. Inorg. Chem. 1995, 34, 4167-4177.
    94301, 94226
  15. Pinkas, J.; Huffman, J. C.; Chisholm, M. H.; Caulton, K. G.: Origin of Different Coordination Polyhedra for Cu[CF3C(O)CHC(O)CF3]2L (L = H2O, NH3). Inorg. Chem. 1995, 34, 5314-5318.
    94348
  16. Tyrlik, S. K.; Kisielinska, M.; Huffman, J. C.: Searching for transition metal coordination compounds, which complex carbohydrates in water solution; synthesis, X-ray crystal structure and u.v.-vis. spectra of oxo-bis[bis-acetonitrile-trichlororuthenium]. Transition Met. Chem. 1995, 20, 413-414.
    94106
  17. Barnhart, D. M.; Clark, D. L.; Gordon, J. C.; Huffman, J. C.; Watkin, J. G.; Zwick, B. D.: Solution Study of the Ambient Temperature Monomer-Dimer Equilibrium Th2(OR)8 = 2Th(OR)4 (R = CH-i-Pr2) and X-ray Crystal Structures of Th2(OCH-i-Pr2)8, Th(OCH-i-Pr2)4(quin), and ThI(OCH-i-Pr2)3(py)2. Inorg. Chem. 1995, 34, 5416-5423.
    91652
  18. Reynolds, J. G.; Sendlinger, S. C.; Murray, A. M.; Huffman, J. C.; Christou, G.: Synthesis and Characterization of Vanadium (II,III,IV) Complexes of Pyridine-2-thiolate. Inorg. Chem. 1995, 34, 5745-5752.
    91014, 91150, 92011
  19. Polynuclear Metal Hydrido Alkoxides. Reactions of W4(H)2(O-i-Pr)14 and W2(H)(O-c-C5H9)7(HNMe2) with Carbon-Carbon, Carbon-Oxygen and Carbon-Nitrogen Multiple Bonds. Barry, J. T.; Chacon, S. T.; Chisholm, M. H.; Huffman, J. C.; Streib, W. E. J. Am. Chem. Soc. 1995, 117, 1974-1990.
    92306, 94012, 91174, 91029, 90374
  20. Dean, N. S.; Bartley, S. L.; Streib, W. E.; Lobkovsky, E. B.; Christou, G.,: Combination of Metal-Metal Bonding and Antiferromagnetic Exchange Interaction in the d2-d2 Complex [V2O(SPh)4(Me2-bpy)2] · THF (Me2-bpy=4,4'Dimethylbipyridine). Inorg. Chem. 1995, 34, 1608-1616.
    91149, 90082
  21. Kuhlman, R.; Streib, W. E.; Caulton, K. G.: Protonation of Chloride in Os(H)2Cl2(PiPr3)2: Synthesis of [(PiPr3)2H2Os(.mu.-Cl)3OsH2(PiPr3)2]CF3SO3. Inorg. Chem. 1995, 34, 1788-1792.
    94124
  22. Chisholm, M. H.; Kramer, K. S.; Streib, W. E.: Complexes with Polar W-W Multiple Bonds: [W2(OiPr)4L(dmpe)2] (L = (H)2, CO) and [W2(O)4(.mu.-O){W(CO)(dmpe)2}2]. Angew. Chem. Intl. Ed. Engl. 1995, 34, 891-893.
    94233, 94102, 92176
  23. Chisholm, M. H.; Kramer, K. S.; Streib, W. E.: [W4(O)2(O-i-Pr)8]2. An Unusual Octanuclear Oxo-Alkoxide Cluster of Tungsten. J. Cluster Sci. 1995, 6, 134-145.
    92195
  24. Budzichowski, T. A.; Chisholm, M. H.; Scheer, M.; Schuster, K.; Streib, W. E.: Is It Possible to stabilise Complexes with a Tungsten-Phosphorous Triple Bond? J. Am. Chem. Soc., Chem. Commun. 1995, 1672-1672.
    93155
  25. Chisholm, M. H.; Folting-Streib, K.; Tiedtke, D. B.; Lemoigno, F.; Eisenstein, O.: Solid-State and Solution Structures of [{NW(OC(CH3)2CF3)3}3] and Factors Favoring the Metathesis of C-N and W-W Triple Bonds in Reactions Involving Organic Nitriles and Ditungsten Hexaalkoxides. Angew. Chem. Intl. Ed. Engl. 1995, 34, 110-112.
    94018
  26. Tsai, H.-L.; Wang, S.; Folting, K.; Streib, W. E.; Hendrickson, D. N.; Christou, G.: High-Spin Molecules: (NBun4)[Mn8O6Cl6(O2CPh)7(H2O)2] (S = 11) and [Mn9Na2O7(O2CPh)15(MeCN)2] (S = 4). J. Am. Chem. Soc. 1995, 117, 2503-2514.
    91135, 91049
  27. Eppley, H. J.; Tsai. H.-L.; De Vries, N.; Folting, K.; Christou, G.; Hendrickson, D. N.: High Spin Molecules: Unusual Magnetic Susceptibility Relaxation Effects in [Mn12O12(O2CEt)16(H2O)3] (S = 9) and the One-Electron Reduction Product (PPh4)[Mn12O12(O2CEt)16(H2O)4] (S = 19/2). J. Am. Chem. Soc. 1995, 117, 301-317.
    92219, 93124
  28. Wemple, M. W.; Adams, D. M.; Folting, K.; Hendrickson, D. N.; Christou, G.: Incorporation of Fluoride into a Tetranuclear Mn/O/RCO2 Aggregate: Potential Relevance to Inhibition by Fluoride of Photosynthetic Water Oxidation. J. Am. Chem. Soc. 1995, 117, 7275-7276.
    94358, 94385
  29. Caulton, K. G.; Chisholm, M. H.; Doherty, S.; Folting, K.: Preparation and Structures of Structures of Arylmolybdenum (6+) Nitrido Compounds: (2,4,6-Me3C6H2)3Mo.tplbnd.N and (2-Me2NCH2C6H4)2(tBuO)Mo.tplbnd.N. Organometallics. 1995, 14, 2585-2588.
    93139, 94048
  30. Kuhlman, R.; Folting, K.; and Caulton, K. G.: An Unusual Example of CH Oxidative Addition following Phosphine Association: Mechanism of Formation and Reactivity of Cp*Ru(.mu.-H)(.mu.-.eta3.,.eta1.-iPrNC(Me)(CHHagostic)RuCp*. Organometallics. 1995, 14, 3188-3195.
    93025
  31. Squire, R. C.; Aubin, S. M. J.; Folting, K.; Streib, W. E.; Hendrickson, D. N.; Christou, G.: Octadecanuclearity in Manganese Carboxylate Chemistry: K4[Mn18O16(O2CPh)22(phth)2(H2O)4] (phthH2 = phthalic acid). Angew. Chem. Int. Ed. Engl. 1995, 34, 887-889.
    94178
  32. Halcrow, M. A.; Streib, W. E.; Folting, K.; Christou G.: Mn6O2{O2C-3,5-(NO2)2-C6H3}10-(C5H5N)2{(CH3)2CO}2].2(CH3)2CO.-2(C2H5)2O and [Mn6O2(O2CC6H5)10-(NCCH3)4]. Acta Crystallogr. 1995, C51, 1263-1267.
    93264, 93151
  33. Dimitrou, K.; Chen, S.-J.; Folting, K.; Christou, G.: The [Co4O4]4+ Cubane as a Quadruply Bridging Unit: The Mixed-Valence Cluster [Co8O4(O2CPh)12(solv)4] (solv = DMF, MeCN, H2O). Inorg. Chem. 1995, 34, 4160-4166.
    93158
  34. Wemple, M. W.; Adams, D. M.; Hagen, K. S.; Folting, K.; Hendrickson, D. N.; Christou, G. J. Am. Chem. Soc.: Site-specific Ligand Variation in Manganese-Oxide Cubane Complexes, and Unusual Magnetic Relaxation Effects in [Mn4O3X(OAc)3(dbm)3] (X = N3-, OCN-; Hdbm = dibenzoylmethane). Chem. Commun. 1995, 1591-1593.
    94248
  35. Eppley, H. J.; Wang, S.; Tsai, H.-L.; Aubin, S. A.; Folting, K.; Streib, W. E.; Hendrickson, D. N.; Christou, G.: High Spin Molecules: A Structural and Magnetic Comparison of High Nuclearity Manganese Carboxylate Aggregates. Mol. Cryst. Liq. Cryst. 1995, 274, 159-166.
    90077, 91049, 91135, 94007, 93232
  36. Tsai, H.-L.; Eppley, H. J.; de Vries, N.; Folting, K.; Christou, G.; Hendrickson, D. N.: High Spin Molecules: Unusual Magnetic Susceptibility Relaxation Behavior of a Dodecanuclear Manganese Aggregate in Two Oxidation States. Mol. Cryst. Liq. Cryst. 1995, 274, 167-173.
    92219, 93232, 93124
  37. Budzichowski, T. A.; Chisholm, M. H.; Folting, K.; Fromhold, M. G.; Streib, W. E.: Metathetic Reactions Involving ditungsten hexapivalate. Preparation and structures of W2(O2CtBu)2(OtBu)2(NiPr2)2, W2(O2CtBu)4(NiPr2)2, W2(O2CtBu)2(OtBu)4 and Na2W4O4Cp2(O2CtBu)6 solvate where Cp = C5H5. Inorg. Chim. Acta. 1995, 235, 339-347.
    93201, 93203, 94046, 92201
  38. Pedersen, A.; Tilset, M.; Folting, K.; Caulton, K. G.: Oxidatively Induced Reductive Elimination from Ru(C2Ph)2(CO)(PtBu2Me)2 and Ru(CHCHPh)(C2Ph)(CO)(PtBu2Me)2. Organometallics, 1995, 14, 875-888.
    93093
  39. Ogasawara, M.; Macgregor, S. A.; Streib, W. E.; Folting, K.; Eisenstein, O.; Caulton, K. G.: Isolable, Unsaturated Ru(0) in Ru(CO)2(PtBu2Me)2: Not Isostructural with Rh(I) in Rh(CO)2(PR3)2+. J. Am. Chem. Soc. 1995, 117, 8869-8870.
    94343
  40. Squire, R. C.; Aubin, S. M. J.; Folting, K.; Streib, W. E.; Christou, G.; Hendrickson, D. N.: Octadecanuclearity in Manganese Carboxylate Chemistry: Preparation and Properties of K4[Mn18O16(O2CPh)22(phth)2(H2O)4] 10 MeCN. Inorg. Chem. 1995, 34, 6463-6471.
    94178
  41. Tyrlik, S.K.; Kisielinska, M.; and Huffman, J.C.: Searching for transition metal coordination compounds, which complex carbohydrates in water solution; synthesis, X-ray crystal structure and u.v.-vis. spectra of oxo-bis[bis-acetonitrile-trichlororuthenium]. Transition Met. Chem. 1995, 20, 413-414.
    94106
  42. Pinkas, J.; Huffman, J.C.; Baxter, D.V.; Chisholm, M.H.; and Caulton, K.G.: Mechanistic Role of H2O and the Ligand in the Chemical Vapor Deposition of Cu, Cu2O, CuO, and Cu3N from Bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)copper(II). Chem. Mater. 1995, 7, 1589-1596.
    94413
  43. Jasper, Jr., S.A.; Huffman, J.C.; and Todd, L.J.: Palladium-Assisted Cyano Substitution Reactions of (Pme2Ph)2Pd(B9H9As2) and (PMe2Ph)2Pd(B9C2H11). X-ray Crystal and Molecular Structures of 5-CN-1,1-(PMe2Ph)2-closo-1,2,3-PdAs2B9H8, 1-tBuNC-5-CN-1-(PMe2Ph)-closo-1,2,3-PdAs2B9H8, and 4,5-(CN)2-1,1-(PMe2Ph)2-closo-1,2,3-PdC2B9H9. Inorg. Chem. 1995, 34, 6430-6439.
    92081, 94181, 93256

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